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 Blotter Spot Test Oil Analysis:VOA Helix HX7 5W30, 16,286 km blotter Shell Helix Ultra 5W40

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Thrust
post Feb 6 2019, 05:55 PM

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A bit free so I want to update you guys on the latest blotter test I've taken from the current Honda Fully Synthetic SN0W30 engine oil as below.

Attached Image @ 3,222KM

Attached Image @ 4622KM

This post has been edited by Thrust: Feb 7 2019, 11:27 AM
TSzeng
post Feb 9 2019, 10:07 AM

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QUOTE(Thrust @ Feb 6 2019, 05:55 PM)
A bit free so I want to update you guys on the latest blotter test I've taken from the current Honda Fully Synthetic SN0W30 engine oil as below.

Attached Image @ 3,222KM

Attached Image @ 4622KM
*
The perimeter ring of centre zone disappears in later blotter spot sample, which is good news indicating detergency/dispersancy properties of this Honda oil is still strong.
Unable to figure out why do earlier 3222 km sample demonstrates some signs of perimeter ring that disappers in longer use ?
Generally later 4622 km sample is more grayish, indicating higher amount of combustion by-products and that's normal for an oil in use longer, IMHO.
Looks like this used Honda 0W30 is good to go for another 2000-4000 km and then see how the blotter spot develops.
Thrust
post Feb 9 2019, 10:14 AM

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QUOTE(zeng @ Feb 9 2019, 10:07 AM)
The perimeter ring of centre zone disappears in later blotter spot sample, which is good news indicating detergency/dispersancy properties of this Honda oil is still strong.
Unable to figure out why do earlier 3222 km sample  demonstrates some signs of perimeter ring that disappers in longer use ?
Generally later 4622 km sample is more grayish, indicating higher amount of combustion by-products and that's normal for an oil in use longer, IMHO.
Looks like this used Honda 0W30 is good to go for another 2000-4000 km and then see how the blotter spot develops.
*
I think I know why there's a perimeter ring on the first (3,222) blotter test. That's because I let the drip of oil dry up without moving it around the paper.

On the 2nd test, I basically turn the paper in a circular motion to spread the oil more evenly.
e-lite
post Feb 9 2019, 09:38 PM

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QUOTE(Thrust @ Feb 9 2019, 10:14 AM)
I think I know why there's a perimeter ring on the first (3,222) blotter test. That's because I let the drip of oil dry up without moving it around the paper.

On the 2nd test, I basically turn the paper in a circular motion to spread the oil more evenly.
*
Your second method is not the correct method. You actually want to see how well the oil can bring particles to the edges. So your second blotter test should be invalid
Thrust
post Feb 10 2019, 07:58 AM

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QUOTE(e-lite @ Feb 9 2019, 09:38 PM)
Your second method is not the correct method. You actually want to see how well the oil can bring particles to the edges. So your second blotter test should be invalid
*
ic... noted on the comment. However, I think different paper quality will also affect on how the oil actually spreads too. So the end result will also depends on what type of paper is being used.

This post has been edited by Thrust: Feb 10 2019, 07:58 AM
TSzeng
post Feb 10 2019, 01:41 PM

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QUOTE(Thrust @ Feb 9 2019, 10:14 AM)
I think I know why there's a perimeter ring on the first (3,222) blotter test. That's because I let the drip of oil dry up without moving it around the paper.

On the 2nd test, I basically turn the paper in a circular motion to spread the oil more evenly.
*
Ok , got it as that circular motion helps to spread out the contaminant particulates (of varying mass/weights) away from the centre zone .

This post has been edited by zeng: Feb 10 2019, 01:42 PM
TSzeng
post Feb 10 2019, 01:44 PM

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QUOTE(e-lite @ Feb 9 2019, 09:38 PM)
Your second method is not the correct method. You actually want to see how well the oil can bring particles to the edges. So your second blotter test should be invalid
*
Concur with your position as I have not read of such 'procedures' being recommended in limited number of webpages online .

This post has been edited by zeng: Feb 10 2019, 01:45 PM
SUSFenix98
post Feb 10 2019, 04:31 PM

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QUOTE(zeng @ Feb 8 2017, 02:03 AM)
What do you think ?
[attachmentid=8469303]
https://bobistheoilguy.com/forums/ubbthread...s_oil_change_up

A1.1) Round 1: Total Quartz 7000 Energy 10W40 SL/A3B4 in 2005 Avanza 1.3L K3-VE
A1.2) Blotters for :12,238 km ; 13,000 km ;13,673 km ; 14,218 km and 16,593 km
Note:Finally oil change at 16,631 km (10,334 miles) in early May 2017 after 9 months in use.
Fuel in use:
Mostly use : (Brand/RON#)  BHP RON 95 ;
Mixed with : (Brand/RON#)  None

A2.1) Round 2: Total Quartz 7000 Energy semi synthetic 10W40 SL/A3B4 in 2005 Toyota Avanza 1.3L K3-VE
A2.2) Blotters for : 5,087 km; 8,665 km ; 10,616 km ; 13,478 km and 15,000 km
Note:On 31 Jan 2018,after 9 months in use,this oil is replaced by fullsyn Shell Helix Ultra 5W40 MB 229.5

A3.1) Round 3: Shell Helix Ultra Full Synthetic 5W40 A3B4,MB 229.5,LL01,VW 50200 50500 in 2005 Toyota Avanza 1.3L K3-VE
A3.2) Blotters for :5575 km;10099 km;14100 km ;17138 km

E1 )Total Quartz 7000 Energy 10W40 semisyn SL A3B4 :-
a)  16,593 km ODO 247k, in  2005 Avanza 1.3 K3VE MPI ;
b) 15,000 km ODO 262k, -ditto-.

Aisin
5W30a )Aisin FS 5W30 (non-PAO) 13536 km and 14990 km  in 2002 Hyundai Elantra 1.8L G4GB @alphaz;

5W40a )Aisin FS (PAO+Ester) 5w-40 SN 12000 km in Elantra 2.0 NA (G4GC),ODO 194k km @speedy3210
Bardahl
5W40a )Bardahl MXP 5W-40 FS 4322 km, ODO 173k;6829 km, ODO 180k in Nissan Livina 1.6 NA @ putra23

Castrol
10W40a )Castrol Magnatec 10W40 SN 1537 km, ODO 234k km in 1999 Proton Wira 1.3 Fuel Injection ;

Honda
0W30a )Honda HMEO Fully Synthetic 0W30 3000 km;4000 km in 2011 Honda City,ODO 101,000 km @ cempedaklife

0W30b )Honda Fully Synthetic 0W30 3750 km in 2011 Honda City,ODO 107,750 km @ cempedaklife

0W30c )Honda Fully Synthetic 0W30 3222 km; 4622 km in 2010 Honda City L15A7,ODO 103k km @ Thrust;

Mobil
15W40a )HDEO Mobil Delvac mineral MX 15W40 (CJ4) 740 km/20 hours of track time, in KTM RC390 Motorcycle @e-lite;

Pennzoil
5W40a )Pennzoil Platinum Velocity 5W40 100%-synthetics 9900 km ,ODO 69k;17000 km, ODO 86k ;22000 km, ODO 91k in 2014 Myvi 1.3 K3VE EFI @Senscents;

Perodua
5W30a )Perodua SS 5W30 SM gold bottle 5000 km,ODO 133k;7000 km;8000 km in Kenari 1.0L @ahsam1212;

PetroCanada
0W30a )HDEO Petro Canada Duron XL 0w30 (API CH4/SJ) synthetic blend, 12707 km  ODO 283k,  in Nissan AD Resort 1.6L GA16 carburettor @chemistry;
15W40a )HDEO Petro-Canada Duron semi synthetic SHP 15w40 (CK4,E9,ECF-3) 11145 km ODO 295k ;12558 km ODO 297k, in Nissan AD Resort 1.6L GA16 carburettor @chemistry;
Petronas
10W40a )Petronas Syntium 800 SS 10W40 SN 4181 km in Toyota Vios NCP 42, Engine: 1NZ-FE ,ODO 189k km @XinG;
Shell
5W30
a )Formula Shell 5W30 "fullsyn"(?) SN GF5, 8500 km ODO 323k, in 1997 Wira 1.5 auto 4G15 carburrettor @Senscents;

b )Shell Helix Ultra Fully Synthetic 5W30 A3B4 (Made in Hong Kong) 10060 km; 14160 km ;15999 km  in 2002 Hyundai Elantra 1.8L G4GB @alphaz

c )Shell Helix HX7 semi synthetic 5W30 SN A3B4 7400 km ODO 60890 km , in Mazda3 @wkc5657

10W40
a )Formula Shell 10W40 mineral SN ,5466 km ODO 395k km, in 1999 Wira 1.6 MPI @speedy3210;

ATF Blotters
Toyota Type IV 32138 km in 2005 Toyota Avanza 1.3 automatic transmission;

UOA/VOA:
VOA Shell Helix Ultra 5W40 (Russia)
Z) Further readings:

On Site Oil & Fluid Analysis
Blotter Spot Test Helps Improve Engine Reliability
Sample Preparation and Test Procedure: A Quick Guide
Evaluating Lubricant Dispersancy
Chromatogram Patterns
Motor Oil Testing On The Cheap
ASTM D7899
Condition-based Lubricating Oil Change
One Drop Instant Lubricant Test
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Where do u buy the chromatographic paper n how much bro ? Been using look at color n sediment in oil for oil changes.... doh.gif

TSzeng
post Feb 10 2019, 09:35 PM

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QUOTE(Fenix98 @ Feb 10 2019, 04:31 PM)
Where do u buy the chromatographic paper n how much bro ? Been using look at color n sediment in oil for oil changes....   doh.gif
*
Hi Fenix98,
Just any A4 letterhead from says bills/statements of TM, banks etc will do .
I've tried A4 with 70gm/80gm printing papers and see no difference.
So called chromatographic paper is difficult to source and may not be necessary, IMO for our purpose.

This post has been edited by zeng: Feb 10 2019, 09:35 PM
jamespaul
post Mar 4 2019, 03:13 PM

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@zeng, What is your take on the limitation of the oil filter?

Say, the manufacturer allows for 10,000km, oil and filter change.

However, based on your expertise, the oil can go further, e.g. 15,000km.

Any change to the oil filter? would that then limit the extension of oil change interval?
TSzeng
post Mar 5 2019, 12:44 PM

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QUOTE(jamespaul @ Mar 4 2019, 03:13 PM)
@zeng, What is your take on the limitation of the oil filter?

Say, the manufacturer allows for 10,000km, oil and filter change.

However, based on your expertise, the oil can go further, e.g. 15,000km.

Any change to the oil filter? would that then limit the extension of oil change interval?
*
Hi Jamespaul,
During 1970/80's , local OEM SC's had been recommending oil filter life of 10,000 km (i.e 2 oil changes @ 5000 km) till todate with use of API SE/SF oils and obsolete manufacturing technology such as 'metal finishing' on contacting components like crankshafts, camshafts, piston rings and piston liners.

As I understand it some (not sure if it's all) Europe VW and MB recommends 30,000 km oil change with Long Life oils like VW 50400 50700, MB 229.5, MB 229.51 etc but not sure about filter change intervals unless some readers can confirm it.

There maybe a 'progressive' OEM SC in KL recommending 15,000 km filter change coinciding with oil change,I don't know and I would like to know if there is any local OEM SC recommending 2X10,000 km or 2X15,000 km filter change.

I'd personally extended filter change to 17,138 km as per my blotter spot tests here with 280k ODO and I strongly believe my blotter is 'clean' enough for extending further filter change interval.

Instead of theorising and speculating on this one may spend chunks of money on UOA and Particle Counts or a cheapo blotter spot test for better 'feel' .

Edit:With my limited knowledge on how oil filter works in our cars, I don't buy the concept of extending oil change interval by replacing oil filter mid way of OCI.
I wouldn't be surprised if 30,000 km filter change interval is recommended in Europe, IDK.

This post has been edited by zeng: Mar 5 2019, 12:58 PM
jamespaul
post Mar 5 2019, 01:20 PM

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QUOTE(zeng @ Mar 5 2019, 12:44 PM)
Hi Jamespaul,
During 1970/80's , local OEM SC's had been recommending oil filter life of 10,000 km (i.e 2 oil changes @ 5000 km) till todate with use of API SE/SF oils and obsolete manufacturing technology such as 'metal finishing' on contacting components like crankshafts, camshafts, piston rings and piston liners.

As I understand it some (not sure if it's all) Europe VW and MB recommends 30,000 km oil change with Long Life oils like VW 50400 50700, MB 229.5, MB 229.51 etc but not sure about filter change intervals unless some readers can confirm it.

There maybe a 'progressive' OEM SC in KL recommending 15,000 km filter change coinciding with oil change,I don't know and I would like to know if there is any local OEM SC recommending 2X10,000 km or 2X15,000 km filter change.

I'd personally extended filter change to  17,138 km as per my blotter spot tests here with 280k ODO and I strongly believe my blotter is 'clean' enough for extending further filter change interval.

Instead of theorising and speculating on this one may spend chunks of money on UOA and Particle Counts or a  cheapo blotter spot test for better 'feel' .

Edit:With my limited knowledge on how oil filter works in our cars, I don't buy the concept of extending oil change interval by replacing oil filter  mid way of OCI.
I wouldn't be surprised if 30,000 km filter change interval is recommended in Europe, IDK.
*
From what I understand, European cars with extended OCI are using Fleece filter, which lasts up to 40,000km. So, they are fine for 15k to 25k km OCI

I understand that Japanese makers are using cellulose or paper, so hence, I was clarifying with you on if this could be the limitation.


Thanks!
TSzeng
post Mar 5 2019, 01:42 PM

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QUOTE(jamespaul @ Mar 5 2019, 01:20 PM)
From what I understand, European cars with extended OCI are using Fleece filter, which lasts up to 40,000km. So, they are fine for 15k to 25k km OCI

I understand that Japanese makers are using cellulose or paper, so hence, I was clarifying with you on if this could be the limitation.
Thanks!
*
Oh yes you're right , MB specifies Fleece filter which is made of 'special' material which isn't paper/cellulose material that I'm talking about .

Hence there should be limitation for cheapo paper filter but whether a certain specific paper filter can do 30000 km?
.... probably not and I don't know for I'm no fan of higher priced 'quality' filter or so called high performance filter.

One thing I learn is OEM's are always too conservative, as UMW Toyata recommends 5000 km oil change for my Avanza.

VW is recommending 30,000 km oil change interval too but I'm not aware it applies to VW OEM filter too.
I'm not sure about VW OEM filter material details .

This post has been edited by zeng: Mar 5 2019, 01:44 PM
wkc5657
post Mar 5 2019, 03:57 PM

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QUOTE(zeng @ Mar 5 2019, 12:44 PM)

I wouldn't be surprised if 30,000 km filter change interval is recommended in Europe, IDK.
*
Not only by using different filter material, but also by increasing the oil sump capacity.

Have read about BMW UK now on 2 year oil change interval, so going towards 3 years is not something surprising.

But, a cautious note is that, if you're driving on lease/fleet/business car, then yes, you can go for such interval levels. As after 3 years, the car is returned and replaced with another car. Whatever possible damage won't likely show up at year 3, but definitely will have very adverse impact beyond 5 years of ownership (like our market).

Also, their driving environment is milder with lesser/shorter jams and moderate driving behaviour plus good quality petrol. This should have favourable impact on oil life also.

So, for us malaysians, for the sake of convenience, keep it to 1 year oil change interval using good synthetic oil within 15,000km is still a good habit.
e-lite
post Mar 5 2019, 07:08 PM

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QUOTE(zeng @ Mar 5 2019, 12:44 PM)
Hi Jamespaul,
During 1970/80's , local OEM SC's had been recommending oil filter life of 10,000 km (i.e 2 oil changes @ 5000 km) till todate with use of API SE/SF oils and obsolete manufacturing technology such as 'metal finishing' on contacting components like crankshafts, camshafts, piston rings and piston liners.

As I understand it some (not sure if it's all) Europe VW and MB recommends 30,000 km oil change with Long Life oils like VW 50400 50700, MB 229.5, MB 229.51 etc but not sure about filter change intervals unless some readers can confirm it.

There maybe a 'progressive' OEM SC in KL recommending 15,000 km filter change coinciding with oil change,I don't know and I would like to know if there is any local OEM SC recommending 2X10,000 km or 2X15,000 km filter change.

I'd personally extended filter change to  17,138 km as per my blotter spot tests here with 280k ODO and I strongly believe my blotter is 'clean' enough for extending further filter change interval.

Instead of theorising and speculating on this one may spend chunks of money on UOA and Particle Counts or a  cheapo blotter spot test for better 'feel' .

Edit:With my limited knowledge on how oil filter works in our cars, I don't buy the concept of extending oil change interval by replacing oil filter  mid way of OCI.
I wouldn't be surprised if 30,000 km filter change interval is recommended in Europe, IDK.
*
You have to take into account that Europe's fuel and engines are designed for Euro 6 already with less sulphur in the fuel. Their oils also call for low ash formulation.

For our Malaysian roads, most of the time our driving falls under "severe" category due to heat and stop & go traffic.
jamespaul
post Mar 6 2019, 03:17 PM

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QUOTE(e-lite @ Mar 5 2019, 07:08 PM)
You have to take into account that Europe's fuel and engines are designed for Euro 6 already with less sulphur in the fuel. Their oils also call for low ash formulation.

For our Malaysian roads, most of the time our driving falls under "severe" category due to heat and stop & go traffic.
*
Since we have high sulphur fuel, we should use full SAPS engine oil.

Depending on the driving scenario.
- if you track your car, yes, the engine oil can exceed operating temperature
- if you are stuck in a jam, but you have a working radiator, operating temperature should remain stable and fine

stop & go traffic isnt that bad, if you maintain your car properly.

From my understanding, "severe" service is for harsh weather, like extreme cold. Our weather are considered good already

Do correct me if I am wrong.
therain01
post Mar 23 2019, 01:43 PM

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I find that the higher the mileage, the less obvious the center ring is on mobil 1 oil. Does that mean the oil detergent works harder at higher mileage? Anyone could enlighten me?

I lost the blotter test sample at mileage below 2000km but I can assure that the center ring was very obvious at lower mileage.


Attached thumbnail(s)
Attached Image Attached Image
TSzeng
post Mar 25 2019, 02:30 PM

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QUOTE(therain01 @ Mar 23 2019, 01:43 PM)
I find that the higher the mileage, the less obvious the center ring is on mobil 1 oil. Does that mean the oil detergent works harder at higher mileage? Anyone could enlighten me?

I lost the blotter test sample at mileage below 2000km but I can assure that the center ring was very obvious at lower mileage.
*
It may be true at times that a higher mileage oil has less obvious centre ring than a lower mileage oil, whether or not it's a Mobil 1.
It appears to me mileage is not the one and only one factor that affects the 'shape' of a blotter spot test, though it's likely the primary one when we look at an oil's 'trending' in a blotter spot test .
Other factors like oil temperature , engine components temperature etc may 'shape' a blotter spot test centre ring other than lighting etc.

Edit:The 7000 km Mobil 1 ESP has indications of fuel dilution phenomenon, is the engine a Turbo direct injection type ?


This post has been edited by zeng: Mar 25 2019, 02:35 PM
therain01
post Mar 25 2019, 08:57 PM

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QUOTE(zeng @ Mar 25 2019, 02:30 PM)
It may be true at times that a higher mileage oil has less obvious centre ring than a lower mileage oil, whether or not it's a Mobil 1.
It appears to me mileage is not the one and only one factor that affects the 'shape' of a blotter spot test, though it's likely the primary one when we look at an oil's 'trending' in a blotter spot test .
Other factors like oil temperature , engine components temperature etc may 'shape' a blotter spot test centre ring other than lighting etc.

Edit:The 7000 km Mobil 1 ESP has indications of fuel dilution phenomenon, is the engine a Turbo direct injection type ?
*
Thanks for the reply. That has been very helpful.

Yes. The mobil 1 ESP 5W30 is on turbo gasoline direct injection engine. Is that normal to have dilution on this type of engine? The sample was taken when the engine is hot after about 1 hour travel.
TSzeng
post Mar 27 2019, 03:03 PM

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QUOTE(therain01 @ Mar 25 2019, 08:57 PM)
Thanks for the reply. That has been very helpful.

Yes. The mobil 1 ESP 5W30 is on turbo gasoline direct injection engine. Is that normal to have dilution on this type of engine? The sample was taken when the engine is hot after about 1 hour travel.
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Gasoline Direct Injection is more prone to fuel dilution problem.
If yours is a certain Japanese or American GDI, I would think it could be 'normal' as some OEM's seems helpless in preempting this problem for some SC's are clueless about the problem and its solution .
European OEM's seems to do better in this .

Anyway looking at your 7000 km blotter and strong specs of M1 ESP 5W30,

Attached Image
I would hazard a guess that it does no harm to the engine at 7000 km, and the oil is still serviceable IMHO.

Edit:BTW, this engine oil spec is recommended for 30,000 km OCI by European MB/VW.

Edit2: Since this 7000 km blotter was taken hot after an hour of travel, it's clear to me the outermost zone points 'solely' to fuel dilution phenomenon.
Most likely it's attributed to being a Gasoline Direct Injection rather than out-of-tune fuel system.

This post has been edited by zeng: Mar 27 2019, 08:26 PM

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