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 Engine Oil Reviews/Technical talk v2, Everything Automotive lubricants/fluids

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TSQuazacolt
post Sep 21 2024, 09:19 PM

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QUOTE(Balanced @ Sep 16 2024, 10:09 PM)
Ah ok. I thought you are importing oils yourself.
*
No

QUOTE(GamersFamilia @ Sep 20 2024, 09:19 PM)
Toyota yaris 1.5 use how many litre of engine oil?
*
2NR-FE ?
should be 3.3+ liters
TSQuazacolt
post Sep 24 2024, 03:36 AM

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2016 GT86 attempted longer intervals
http://www.quazacolt.com/uoa/others/202403...OIL_SS_0w30.png
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Virgin oil Analysis! (VOA) YES! MIZU!
http://www.quazacolt.com/uoa/others/202406..._Semi_10w40.png
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http://www.quazacolt.com/uoa/others/202311..._Proton_CVT.png
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My own GT86 back to back reports trying out new Valvoline SynPower Eco , next up, trying out MoS2! additives
http://www.quazacolt.com/uoa/gt86/20240311...line_Eco_01.png
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http://www.quazacolt.com/uoa/gt86/20240614...line_Eco_02.png
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some Q&A for my own samples:
1) Does wear in general increase exponentially? Reason for this is that my latest 2 samples did not run half as much compared to the previous Petronas, however the wear is indeed half in general.
Wear metals normally increase as the oil is run longer. Iron tends to change depending on the kilometers on the oil the most directly. Your iron levels on these two reports are indeed lower than the levels on the three reports before them, even when you divide the parts per million by the kilometers on the oil. In spite of the increase in spirited driving you mentioned on the information sheet with the sample, steel parts are truly wearing less than they had been.

2) This Valvoline is very intriguing that, it is a very slightly thinner oil, lesser shown additive package with lower, just about everything (moly/ZDDP etc) compared to the Petronas, seems to be on cheaper Group 3 base oils, with an Eco labeling seemingly for Asian or Emerging markets: https://www.valvolineglobal.com/en-th/synpower-eco-0w-20/ (in future samples please correct the Oil Type and Grade info) the website is pointed to Thailand, and the oil is made in Singapore. Our distributor in Malaysia does import it, but not widely marketed yet. Said Malaysian distributor website is still on the old "non eco" SynPower https://greatoceanauto.com.my/product/valvo...npower-sn-plus/ no actual API donut/cert and EOLCS also shows the same: https://engineoil.api.org/Directory/EolcsRe...ame%3DValvoline
I will create a new oil type in our system specific to SynPower Eco 0W/20. The "should-be" values for the oil's physical properties will be the same as what we have for the"non-eco" SynPower 0W/20. If you think they should be different, let me know, and I will look into changing them. The link to the Eco product you shared clearly shows the API donut sticker and API SP on the front of the bottle. The API license you linked to has the effective date 01 April, 2024; maybe this particular brand was brought to market after that date, and that is why it is not listed on the license. Regardless, the results suggest this oil has performed very well in your engine.

3) In relation to question 1 and 2, why does Valvoline perform better?
I do not know why you have less steel wear with this Valvoline oil than you were getting with Petronas.

4) How is my thought process that this current Valvoline being lower on Moly, adding Liqui Moly MoS2 additive should generally be only positives with no downside besides the additional cost?
It would be hard to get better results than these, so I would not expect any positive changes from adding Liqui Moly MoS2 additive. It should not hurt to add it if you want to, though.

5) Does MoS2 contribute to LSPI?
I have not seen any research linking MoS2 additive to LSPI.

follow up corresponding email

I have learned some things about MoS2 and LSPI... but not enough to draw a conclusion. This doctoral thesis is the most comprehensive study on LSPI that I have seen that is available for free. The section that is relevant to oil formation is on page 26, which cites several other research articles that have been done on the topic with very interesting findings, including some conflicting information about the impact of Molybdenum additives. I do not usually send links to scholarly articles to our customers, but I have a feeling you will appreciate it! If not, that is okay too smile.gif

https://cris.brighton.ac.uk/ws/portalfiles/...rvey_Thesis.pdf


This post has been edited by Quazacolt: Sep 24 2024, 11:59 AM
TSQuazacolt
post Sep 24 2024, 04:24 AM

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goldfries / empire23

I'm going to run out of first page posts soon available for [img] tagging.

how do i work around the [img] tag limitation?
just posting img link without tagging it as image?
TSQuazacolt
post Feb 10 2025, 09:00 AM

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QUOTE(ayamxxx @ Feb 10 2025, 08:51 AM)
But always start it warm up once weekly, cz if not start for too long can diminish the engine oil.
*
If you do not warm up/drive it long enough to at least reach 90c temps, you're better off leaving it cold storage never start up.

Otherwise, You'll do more harm than good through fuel dilution.
TSQuazacolt
post Feb 10 2025, 10:35 AM

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QUOTE(DM3 @ Feb 10 2025, 10:31 AM)
Wat if idling start but rev gradually off n on for about 10mins?
*
No good

Most cars needs between 20-30 minutes of idling even in Malaysian weather to get to 90c

If you drive right away normally, you can cut that time down by at least 5 to 10 minutes+ so at least still need between 10-25 of driving to get 90c (operating temp, and hot enough to prevent fuel dilution)
TSQuazacolt
post Feb 10 2025, 04:03 PM

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QUOTE(Iceman74 @ Feb 10 2025, 01:08 PM)
ohmy.gif  so short lifespan?

me now not too sure want to change EO when and with Semi or Fully
last time fully and now it time to change again
*
just go with fully synthetic, reputable brands, can be gotten for cheap.
and for your application, can definitely be more value than mineral/semi

oil change between 6 months to 1 year is fine.
TSQuazacolt
post Feb 17 2025, 05:32 AM

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Back with our Honda Integra this time using Motul 300v
the additive package is quite interesting in this 300V, especially the Moly, more than doubled even my purposeful additional additive usage confused.gif
https://www.quazacolt.com/uoa/others/202410..._Motul_300v.png
» Click to show Spoiler - click again to hide... «


i think this is our first BMW 320D oil sample here?
Can't remember if we had diesel UOA shared before
https://www.quazacolt.com/uoa/others/202412...hevron_Delo.jpg
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Proton Iriz CVT after numerous Sepang track days and Touge
https://www.quazacolt.com/uoa/others/20241227_Iriz_cvt.jpg
» Click to show Spoiler - click again to hide... «


2016 GT86 trying out adding 2T oil during refuels
Yes Blackstone misunderstood it as 2 tablespoons of fuel into the oil laugh.gif
https://www.quazacolt.com/uoa/others/202411...ite_Racing5.jpg
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My own GT86 with Valvoline SynPower Eco 0w20 and now with Tan Chong MoS2 additives,
strangely... it seemed that visually black MoS2 only amounted to just...less than 200 moly PPM...?
https://www.quazacolt.com/uoa/gt86/20241014...Eco_mos2_01.jpg
» Click to show Spoiler - click again to hide... «

no Q&A yet as it's been a bit slow for the folks at Blackstone labs. maybe through winter cold and going through changes with their new president laugh.gif

This post has been edited by Quazacolt: Feb 17 2025, 11:28 AM
TSQuazacolt
post Feb 19 2025, 11:34 AM

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QUOTE(outpace @ Feb 19 2025, 10:58 AM)
oil added for Jason's Subaru, does it mean before the final oil change, he added a lot of engine oil (500ml / 700 ml) ?
So adding 2T into our four stroke engine is  thumbup.gif ? especially for hot spirit drive ? better protection than RON100 or vpower  ?
*
I've topped up twice within my oil interval to finish up 6 liters

No idea on my friend 2T usage, I don't drive his car enough to be able to properly assess.

I'm only using RON95, to my knowledge he too

This post has been edited by Quazacolt: Feb 20 2025, 07:41 AM
TSQuazacolt
post Feb 23 2025, 05:13 PM

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QUOTE(Quazacolt @ Feb 17 2025, 05:32 AM)
Back with our Honda Integra this time using Motul 300v
the additive package is quite interesting in this 300V, especially the Moly, more than doubled even my purposeful additional additive usage  :confused:
https://www.quazacolt.com/uoa/others/202410..._Motul_300v.png
» Click to show Spoiler - click again to hide... «


i think this is our first BMW 320D oil sample here?
Can't remember if we had diesel UOA shared before
https://www.quazacolt.com/uoa/others/202412...hevron_Delo.jpg
» Click to show Spoiler - click again to hide... «


Proton Iriz CVT after numerous Sepang track days and Touge
https://www.quazacolt.com/uoa/others/20241227_Iriz_cvt.jpg
» Click to show Spoiler - click again to hide... «


2016 GT86 trying out adding 2T oil during refuels
Yes Blackstone misunderstood it as 2 tablespoons of fuel into the oil laugh.gif
https://www.quazacolt.com/uoa/others/202411...ite_Racing5.jpg
» Click to show Spoiler - click again to hide... «

My own GT86 with Valvoline SynPower Eco 0w20 and now with Tan Chong MoS2 additives,
strangely... it seemed that visually black MoS2 only amounted to just...less than 200 moly PPM...?
https://www.quazacolt.com/uoa/gt86/20241014...Eco_mos2_01.jpg
» Click to show Spoiler - click again to hide... «

no Q&A yet as it's been a bit slow for the folks at Blackstone labs. maybe through winter cold and going through changes with their new president laugh.gif
*
Q&A
I'm interested to find out more about Molybdenum / MoS2 - how can we tell if the additive is on basic moly or the latest tri-nuclear moly?

I'm curious about my friend's Integra oil sample as his 300V has more Moly compared to my Moly additive, i still have 300less ppm compared to his moly that's originally in the 300v engine oil itself.
QUOTE
That is not something we can tell you. You would have to find a lab that can identify those specific compounds.


I've also noticed the increased in viscosity and flash point.
Considering my application that the car will see higher RPM/load/stress:
1) would the thicker oil offer better protection?
2) is the changes caused by the MoS2 additive treatment? (Such as the additive carrier oil)
3) would this MoS2 additive usage be considered positive , negligible, or even negative?
QUOTE
I do not think the change in viscosity is very significant, and I do not know of any correlation between MoS2 additive. However, that doesn't mean there is no correlation - only that I have not seen it, and it's not a known issue here at the lab. Some additives (like Lucas oil treatment) can cause the oil to thicken, but I have not seen that with MoS2.

In theory, thicker oil should better protect the bearings. But I do not think that the change we saw in this sample's viscosity is significant enough to really have any effect. The viscosity read about the same several samples back, and wear metals were pretty much the same as they are now.

If you like the additive, feel free to keep using it. From what I can see here, it's not having any significant effect. But sometimes people will report that they used something and it made the engine easier to start, or it quieted down a knock, or they get better mileage - all things we can't see in analysis. So if you like it, it's fine to use. I just don't see it having any effect on how the engine is wearing. Your FA20 looks like a really nice engine that's going to wear well regardless of any additives you decide to use.

TSQuazacolt
post Apr 14 2025, 12:56 PM

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finally. lol.
TSQuazacolt
post Jul 4 2025, 06:52 AM

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Proton Iriz CamPro engine after numerous Sepang track days and Touge
https://www.quazacolt.com/uoa/others/202412...etronas3000.png
» Click to show Spoiler - click again to hide... «

second follow up sample
https://www.quazacolt.com/uoa/others/202505...etronas3000.png
» Click to show Spoiler - click again to hide... «




My own GT86 with Valvoline SynPower Eco 0w20 and now with Tan Chong MoS2 additives ,
Moly (MoS2) very slight increase with continual usage
https://www.quazacolt.com/uoa/gt86/20250311...ineEco_MoS2.png
» Click to show Spoiler - click again to hide... «


Finally! first Mobil 1 SHC 75w90 gear oil sample!
https://www.quazacolt.com/uoa/gt86/20250115...0_Mobil1SHC.png
» Click to show Spoiler - click again to hide... «


My First LSD sample, using Motul Gear 300 LS 75w90
https://www.quazacolt.com/uoa/gt86/20250115...ulGear300LS.png
» Click to show Spoiler - click again to hide... «


no Q&A yet as Blackstone labs getting even slower, lol.
not to mention various typos and errors compared to information provided from my oil slips. (all 3 reports also contained typos and errors)

This post has been edited by Quazacolt: Jul 7 2025, 12:15 PM
TSQuazacolt
post Jul 13 2025, 02:46 PM

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QUOTE(zDestinyx @ Jul 13 2025, 01:52 PM)
I am actually quite surprised seeing that Syntium 3000 actually consists of Molybdenum. Seems like it becomes an important friction modifier for engine oil nowadays for improving fuel consumption and reduce wear.

Notice the previous sample of Valvoline SynPower 0w20 has more insoluble (0.4% vs 0.2% in the latest UOA). Possible is it due to the MoS2 additive? As MoS2 itself is a solid lubricant and the particles are just suspended in the base oil of the additive. Hence, under the continuous usage of the oil and the MoS2 gone through heat and pressure, it coated to the internal parts of the engine and breaks down from its solid counterpart. End up the increases in Moly level and reduce in insoluble content.

Just wonder if the sulphur from the MoS2 will affect the TBN number or not? As the test doesn't show the TBN and TAN.
*
Molybdenum is very popular these days because it's one those additives that doesn't have any obvious detrimental issues.

The only problem is that they aren't like zinc or phosphorus that's able to cling to metal surfaces. Hence their benefits are also very limited.

Another "issue" is how there's differences in MoS2 similarly to base oil
https://bobistheoilguy.com/forums/threads/w...ar-moly.314523/
I'm not sure if there's any tests or analysis that can determine or differentiate the various MoS2 types.
(Base oil you can)

The insolubles are negligible and it's apart of my previous Q&A and recent Q&A/notes
Regardless, you can also refer to
https://www.blackstone-labs.com/all-about-insolubles/
Basically, the MoS2 are smaller microns than the test, as well as oil filter. (Otherwise they are all caught by the filter and just clog it up)

I've got enough data of TBN so didn't pay extra for it
But through experience and also my previous report, no it doesn't affect TBN
TSQuazacolt
post Jul 13 2025, 10:03 PM

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QUOTE(zDestinyx @ Jul 13 2025, 03:32 PM)
I think the Moly appears in modern engine oil nowadays are so called "soluble moly" or "organic moly" such as MoDTC or MoDTP.
Meanwhile, MoS2 considers as insoluble moly which is why it is in grey colour due to the nature of the solid particles suspended.
That's what my limited understanding on Moly.

The MoS2 actually binds to the metal through the sulfur atom, but perhaps not as strong as ZDDP binding to the metal parts of engine.
https://www.imoa.info/molybdenum-uses/molyb.../lubricants.php
*
I don't have any way to tell as sulphur is not tested for all my samples from Blackstone labs.

I would like to think Sulphur is added minimally considering the potential issue on oil becoming acidic (faster), and/or cat con poisoning.

And of course, the EU low SAPS agenda.
But I could be wrong since the MoS2 engine oil additive I've been using (also 2 sample reports done, 3rd Sample with Penrite and Sepang track day is coming very soon!) is by Tan Chong, and may very well ignore any EU regulations, despite it's been OEM/produced by Liqui Moly Germany.

Yes the additive is indeed in very dark grey/black colour. Visibly very powdery.


QUOTE(VeeJay @ Jul 13 2025, 07:29 PM)
As for Bardhal, C60, it uses MoDTC but coupled with polysulphide complex, as the other layer. Am I correct it the presumption?
*
No idea with Bardhal. Never looked into that brand.
TSQuazacolt
post Jul 16 2025, 04:44 PM

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QUOTE(Quazacolt @ Jul 4 2025, 06:52 AM)
Proton Iriz CamPro engine after numerous Sepang track days and Touge
https://www.quazacolt.com/uoa/others/202412...etronas3000.png
» Click to show Spoiler - click again to hide... «

second follow up sample
https://www.quazacolt.com/uoa/others/202505...etronas3000.png
» Click to show Spoiler - click again to hide... «

My own GT86 with Valvoline SynPower Eco 0w20 and now with Tan Chong MoS2 additives ,
Moly (MoS2) very slight increase with continual usage
https://www.quazacolt.com/uoa/gt86/20250311...ineEco_MoS2.png
» Click to show Spoiler - click again to hide... «


Finally! first Mobil 1 SHC 75w90 gear oil sample!
https://www.quazacolt.com/uoa/gt86/20250115...0_Mobil1SHC.png
» Click to show Spoiler - click again to hide... «


My First LSD sample, using Motul Gear 300 LS 75w90
https://www.quazacolt.com/uoa/gt86/20250115...ulGear300LS.png
» Click to show Spoiler - click again to hide... «


no Q&A yet as Blackstone labs getting even slower, lol.
not to mention various typos and errors compared to information provided from my oil slips. (all 3 reports also contained typos and errors)
*
Finally Q&A from my end

Engine
1) Can we consider the up trend of aluminium and iron be related to the Moly additives? or just a negligible difference that's probably just from the slight increase of mileage ran?
I think this is more just a negligible difference based on changes in mileage/use.

2) What does Trace (TR) mean in the report? Specifically, what % of fuel is present as opposed to a number value of previous samples such as <0.5? Or is it a binary value "yes or no" that is either trace or below 0.5?
It means "trace" — not enough to quantify. So, yes, there's fuel present, but the way we measure fuel, we can't get precise enough to say how much.

3) Would throttle body cleaners contribute to fuel trace?
I'm not entirely sure. Depends on when you used them and how much you used, I would guess... but this isn't something that, to my knowledge, we've isolated as a variable and tested.

4) From what I've mentioned in the notes, would the increased Silicon be a result of the vacuum leak?
It could be, sure.


Manual Transmission
1) What does Boron and Magnesium do for transmission additives?
I'm not entirely sure. In engine oils they serve as anti-wear/anti-corrosion additives and detergent/dispersant additives, but I don't know that we know for sure what purpose they serve in transmission fluid. Might be the same purpose.

2) Considering the additives are quite identical, the only difference between Mobil and Motul is just the base oil?
I don't know that I'd call them identical, but very, very similar. There could be other things that are different between them — things we don't test. Like, for example, the base stock of the oil.

3) Does Blackstone Labs have any tests that can identify any samples's base oil?
Not at this time.


Rear Differential / LSD
1) As this is my first rear differential sample, and the car was manufactured in 2013, with a significant amount of mileage, it seems like the differential is still kinda running in from the wear trend? (nickel / silicon amount)
I'm not sure — I guess it depends on how many oil changes have been done. If it's been more than a couple oil changes, I wouldn't expect this metal to still be from wear-in.

2) My friend's previous report highlighted a lot more Nickel as I was slightly worried, and referred to his report [omit]
His unit was considerably newer; probably that was a break-in sample.

3) It does beg the question: Why do the universal averages differ quite a bit from both our differential sample reports? It's as if the universal average does not contain nickel at all while ours have a lot more.
Because our differential average files aren't as precise as what the engine average files are. Most people have no idea of the make/model of their differential, so anything that comes with a Toyota name is put together in the average file — Anything from Tundras and other pickup trucks to sportier cars. It would be ideal if we separated the units out a bit more and had precise averages, but we don't see as many differential samples as we do engine oil samples, so the number of samples (and the lack of information about the samples) prevents more specific averages from being created.

4) My friend's (assuming) factory fill seemed a lot thinner. How much does viscosity contribute in reducing wear?
I don't know that it does, necessarily. For differentials, this isn't something we've explored a lot. We've explored it a bit more in engine oil samples just because we get so many more engine oil samples than differential samples, so there's enough data to come up with some meaningful reults. Also, the frequency of sampling engine oil vs differential samples lends itself to a bit more comprehensive examination. It's hard with differentials when they're only sampled every 30,000 miles — and sometimes they're only sampled once or twice within a vehicle's life. It's hard to get any hard-and-fast data on how viscosity affects wear patterns.

5) Considering probably the only downside for thicker viscosity oils in a Torsen differential is only fuel consumption or efficiency, if reducing wear is the goal, just go as thick as possible?
I don't know; we don't have enough data to say. (see previous question)
TSQuazacolt
post Jul 22 2025, 10:54 AM

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QUOTE(zDestinyx @ Jul 20 2025, 02:00 AM)
Noted. Thanks for your input.

Just curious, I notice Valvoline Malaysia doesn't seem to bring in SynPower Eco 0w20. The one that able to be found from official is just SynPower 0w20 without the Eco labelling.
Mind to share where you get it from? Kind of interested in their oil especially the new Restore and Protect. Too bad, seems like Valvoline Malaysia not yet bring it in.
*
yeah i find it weird myself too as i never noticed that eco labeling Valvoline in Malaysia.
closest thing i found is Valvoline Thailand lol

i got it directly through a friend, through direct distributor or uh partnership?
https://greatoceanauto.com.my/valvoline-partnership/

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